Virtual Textbook of Analytical Chemistry

The following web-sites provide a on-line resources for students, and teachers.  In the changing scenario of Internet world all the information are available at the tip of figure. Attempts have, therefore, been made to make available the power point presentations of different topics of analysis.  This article is based on a presentations made by me for the daily class teaching to Pharmacy students. This will help the students to attempt to keep ahead of lectures in their text reading.

My lecture notes will be at least some extent to be on-line throughout the year. However, note the following
U. A. Deokate (M.Pharm.)
    Comments, questions and errors should be sent to deokate@yahoo.com

Table of Contents

This index provides an introduction to some of the fundamental concepts and methods of analytical chemistry. The topics are arranged in the order in which they are commonly presented in an undergraduate analytical chemistry course.

Theory lecturers of Analysis : new.gif (2364 bytes) (Newly edited classroom presentations)

1. Introduction - A brief introduction to analytical chemistry and analytical methods.
2. Optical Method of analysis - Introduction to optical methods of analysis, EMR, characteristics of EMR, electromagnetic spectrum
3. Introduction to Absorption spectroscopy - Introduction to absorption spectroscopy with descriptions of absorption, emission, scattering, and links to the Beer-Lambert Law and advanced examples.
4. General Instrumentation for Optical spectroscopy - Introduction to general components of optical spectroscopy
5. Statistical Treatment of Analytical Data - Definitions of accuracy and precision, and the basics of significant figures and statistics
6. Laboratory training module - Basic laboratory training module
7. UV-Visible spectroscopy - Introduction, Principal of UV-visible spectroscopy, electronic transactions involved in it.
8.
Woodward-Fieser Rules
 - Application of woodward Fieser rule for calculations of Lambda max position.
9. I.R. Spectroscopy   Introduction, Principal of IR spectroscopy, theory, Vibration transaction involved Instrumentation etc.
10. Fluorescence and Phosphorescence spectroscopy   Introduction, Principal Instrumentation and applications
11. Flame Emission spectroscopy   Introduction, Principal Instrumentation and applications
12. NMR Spectroscopy   Introduction, Principal Instrumentation and applications
13. Mass spectroscopy   Introduction, Principal Instrumentation and applications
14. Chromatography (Introduction)   Definitions, Classification and types of Chromatography
15. Thin Layer Chromatography   Introduction, Principal Instrumentation and applications
16. Column chromatography   Introduction, Principal Instrumentation and applications
16. Gas chromatography   Introduction, Principal Instrumentation and applications
17. Gravimetric analysis   Introduction, Principal Instrumentation and applications

Chars of Analysis Practicals: (Laboratory charts)

Instrumental methods (P.A. II)

Exp. No.1 - Determine the strength of given hydrochloric acid using PH metric titration
Exp. No.2 -

Determine the pKa Value of given acid using PH meter.

Exp. No.3 - Determine the Formal Redox Potential of Ferrous Sulphate using Potentiometric titration
Exp. No.4 - Determine the strength of given hydrochloric acid using conductometric titration
Exp. No.5 -

Determine the strength of given mixture of  acid (HCl, Acetic acid) using Conductometric  titration

Exp. No.6 -

To find out Specific Rotation and Determination of Concentration of Dextrose Injection I.P
Exp. No.7   Estimation of Potassium by Flame Photometry.
Exp. No.8   Selection of filter (lmax) for KMnO4 / K2Cr2O7 by colorimetric measurement.
Exp. No.9   Verify Beer’s law of colorimetric measurement and to find out the unknown concentration of given sample of KMO4
Exp. No.10   Estimation of Quinine Sulfate by Flurometry.

Chemical  methods (P.A. I)

Exp. No.1 - Basic Tool And Operation In Analytical  Chemistry. Titration Tips
Exp. No.2 -

Calibrations of glass wares used in pharmaceutical analytical chemistry laboratory.
Exp. No.3 -

Preparation and standardization of 0.1M sodium Hydroxide solution  I.P.
Exp. No.5 -

Preparation and standardization of 0.1M Hydrochloric acid solution  against sodium carbonate.

Exp. No.6

To determine the percentage purity of given sample of Boric Acid I.P.
Exp. No,7

To determine the percentage purity of given sample of Aspirin I.P.
Exp. No.8

Preparation and standardization of 0.1N KMnO4 solution against sodium Oxalate

Exp.No.9 Determination of percentage purity of ferrous sulphate
Exp. No. 10

Preparation and standardization of 0.05M Iodine solution against Arsenic trioxide 

Exp. No.11 Determination of percentage purity of ascorbic acid I.P

 

Copyright © by U. A. Deokate, all rights reserved.

Last edited on: Thursday, 03 June 2010 07:31:41 PM +0530